Information card for entry 7158127

Structure parameters

• Formula: C27 H24 N S Sb
• Calculated formula: C27 H24 N S Sb
• Title of publication: Direct Sb‒S cross-coupling of halostibines with thiols and disulfides at room temperature
• Authors of publication: Li, Wei; Li, Shan; Wang, Zixiu; Liu, Chenfu; Ye, Yifei; Chen, Yujing; Xiong, Yuyan; lei, jian
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2021
• a: 11.9614 ± 0.0005 Å
• b: 15.2361 ± 0.0007 Å
• c: 12.3334 ± 0.0005 Å
• α: 90°
• β: 92.953 ± 0.004°
• γ: 90°
• Cell volume: 2244.72 ± 0.17 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.0665
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No