Information card for entry 7158128

Structure parameters

• Formula: C26 H28 N S Sb
• Calculated formula: C26 H28 N S Sb
• SMILES: [Sb]12(Sc3ccccc3)[N](Cc3c1cccc3)(C1CCCCC1)Cc1ccccc21
• Title of publication: Direct Sb‒S cross-coupling of halostibines with thiols and disulfides at room temperature
• Authors of publication: Li, Wei; Li, Shan; Wang, Zixiu; Liu, Chenfu; Ye, Yifei; Chen, Yujing; Xiong, Yuyan; lei, jian
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2021
• a: 8.7657 ± 0.0006 Å
• b: 19.2142 ± 0.0013 Å
• c: 13.3556 ± 0.0009 Å
• α: 90°
• β: 101.451 ± 0.007°
• γ: 90°
• Cell volume: 2204.7 ± 0.3 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0939
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No