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Information card for entry 7158591
Preview
Coordinates | 7158591.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C30 H22 N2 O3 S |
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Calculated formula | C30 H22 N2 O3 S |
Title of publication | Sulphur ylide-mediated cyclopropanation and subsequent spirocyclopropane rearrangement reactions. |
Authors of publication | Dai, Qing-Song; Li, Jun-Long; Wang, Qi-Wei; Yang, Si-Lin; Tao, Ying-Mao; He, Mei-Hao; Li, Qing-Zhu; Han, Bo; Zhang, Xiang |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2022 |
Journal volume | 20 |
Journal issue | 17 |
Pages of publication | 3486 - 3490 |
a | 21.023 ± 0.003 Å |
b | 12.4076 ± 0.0016 Å |
c | 18.781 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 4898.9 ± 1.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 5 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for all reflections | 0.0583 |
Residual factor for significantly intense reflections | 0.0422 |
Weighted residual factors for significantly intense reflections | 0.0929 |
Weighted residual factors for all reflections included in the refinement | 0.1018 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7158591.html
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Users of the data should acknowledge the original authors of the
structural data.