Information card for entry 7158592
| Formula |
C28 H20 N2 O3 S2 |
| Calculated formula |
C28 H20 N2 O3 S2 |
| Title of publication |
Sulphur ylide-mediated cyclopropanation and subsequent spirocyclopropane rearrangement reactions. |
| Authors of publication |
Dai, Qing-Song; Li, Jun-Long; Wang, Qi-Wei; Yang, Si-Lin; Tao, Ying-Mao; He, Mei-Hao; Li, Qing-Zhu; Han, Bo; Zhang, Xiang |
| Journal of publication |
Organic & biomolecular chemistry |
| Year of publication |
2022 |
| Journal volume |
20 |
| Journal issue |
17 |
| Pages of publication |
3486 - 3490 |
| a |
11.4722 ± 0.0009 Å |
| b |
11.6024 ± 0.0009 Å |
| c |
11.81 ± 0.0011 Å |
| α |
112.336 ± 0.003° |
| β |
91.537 ± 0.003° |
| γ |
112.501 ± 0.003° |
| Cell volume |
1315.8 ± 0.2 Å3 |
| Cell temperature |
185 ± 2 K |
| Ambient diffraction temperature |
185 K |
| Number of distinct elements |
5 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0841 |
| Residual factor for significantly intense reflections |
0.0503 |
| Weighted residual factors for significantly intense reflections |
0.1188 |
| Weighted residual factors for all reflections included in the refinement |
0.1357 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.028 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7158592.html
