Information card for entry 7158795
Formula |
C28 H24 Cl N O2 S Se2 |
Calculated formula |
C28 H24 Cl N O2 S Se2 |
Title of publication |
Synthesis of 1,2-diselenides via potassium persulfate mediated diselenation of allenamides with diselenides. |
Authors of publication |
Tan, Xiao-Ju; Zhao, Kun; Zhong, Xue-Fang; Yang, Lan; Dong, Yi-Ming; Wang, Tian-Mi; Yu, Shengping; Zhao, Zhi-Gang; Li, Xiao-Xiao |
Journal of publication |
Organic & Biomolecular Chemistry |
Year of publication |
2022 |
a |
8.797 ± 0.0007 Å |
b |
9.5081 ± 0.001 Å |
c |
31.917 ± 0.003 Å |
α |
90° |
β |
90° |
γ |
90° |
Cell volume |
2669.6 ± 0.4 Å3 |
Cell temperature |
303 ± 2 K |
Ambient diffraction temperature |
303 K |
Number of distinct elements |
7 |
Space group number |
19 |
Hermann-Mauguin space group symbol |
P 21 21 21 |
Hall space group symbol |
P 2ac 2ab |
Residual factor for all reflections |
0.0707 |
Residual factor for significantly intense reflections |
0.0321 |
Weighted residual factors for significantly intense reflections |
0.0649 |
Weighted residual factors for all reflections included in the refinement |
0.0716 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.02 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/7158795.html