Information card for entry 7158796
| Formula |
C30 H28 Cl N O2 S Se2 |
| Calculated formula |
C30 H28 Cl N O2 S Se2 |
| Title of publication |
Synthesis of 1,2-diselenides via potassium persulfate mediated diselenation of allenamides with diselenides. |
| Authors of publication |
Tan, Xiao-Ju; Zhao, Kun; Zhong, Xue-Fang; Yang, Lan; Dong, Yi-Ming; Wang, Tian-Mi; Yu, Shengping; Zhao, Zhi-Gang; Li, Xiao-Xiao |
| Journal of publication |
Organic & Biomolecular Chemistry |
| Year of publication |
2022 |
| a |
10.5442 ± 0.0004 Å |
| b |
11.6339 ± 0.0005 Å |
| c |
11.9876 ± 0.0006 Å |
| α |
97.872 ± 0.002° |
| β |
101.392 ± 0.002° |
| γ |
91.286 ± 0.002° |
| Cell volume |
1426.11 ± 0.11 Å3 |
| Cell temperature |
150 ± 2 K |
| Ambient diffraction temperature |
150 K |
| Number of distinct elements |
7 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0625 |
| Residual factor for significantly intense reflections |
0.0421 |
| Weighted residual factors for significantly intense reflections |
0.1011 |
| Weighted residual factors for all reflections included in the refinement |
0.1098 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.062 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7158796.html
