Information card for entry 7201040

Structure parameters

• Formula: C27 H70 Ge Mo12 N11 Ni4 O47
• Calculated formula: C27 H56 Ge Mo12 N11 Ni4 O45
• Title of publication: The first ε-Keggin core of molybdogermanate in extended architectures of nickel(II) with N-donor ligands: syntheses, crystal structures and magnetic properties
• Authors of publication: Wang, Wenju; Xu, Lin; Gao, Guanggang; Liu, Li; Liu, Xizheng
• Journal of publication: CrystEngComm
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 11
• Pages of publication: 2488
• a: 14.544 ± 0.002 Å
• b: 15.039 ± 0.003 Å
• c: 18.655 ± 0.003 Å
• α: 112.528 ± 0.003°
• β: 106.237 ± 0.003°
• γ: 97.703 ± 0.002°
• Cell volume: 3482.3 ± 1 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1017
• Residual factor for significantly intense reflections: 0.0574
• Weighted residual factors for significantly intense reflections: 0.129
• Weighted residual factors for all reflections included in the refinement: 0.1551
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No