Information card for entry 7201041

Structure parameters

• Formula: C30 H66 Ge Mo12 N11 Ni4 O42
• Calculated formula: C30 H62 Ge Mo12 N11 Ni4 O42
• Title of publication: The first ε-Keggin core of molybdogermanate in extended architectures of nickel(II) with N-donor ligands: syntheses, crystal structures and magnetic properties
• Authors of publication: Wang, Wenju; Xu, Lin; Gao, Guanggang; Liu, Li; Liu, Xizheng
• Journal of publication: CrystEngComm
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 11
• Pages of publication: 2488
• a: 33.91 ± 0.006 Å
• b: 15.219 ± 0.003 Å
• c: 26.76 ± 0.005 Å
• α: 90°
• β: 103.472 ± 0.003°
• γ: 90°
• Cell volume: 13430 ± 4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0813
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1319
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No