Information card for entry 7201604

Structure parameters

• Formula: C68 H106 N102 O17 Zn17
• Calculated formula: C68 H74 N102.02 O17 Zn17
• Title of publication: The crystal structures of four azido-bridged Zn(ii) complexes based on open-chain diazine Schiff-base ligands
• Authors of publication: Yue, Yan-Feng; Gao, En-Qing; Fang, Chen-Jie; Zheng, Tao; Liang, Jue; Yan, Chun-Hua
• Journal of publication: CrystEngComm
• Year of publication: 2008
• Journal volume: 10
• Journal issue: 5
• Pages of publication: 614
• a: 13.5903 ± 0.0004 Å
• b: 15.1186 ± 0.0006 Å
• c: 18.8621 ± 0.0007 Å
• α: 101.383 ± 0.002°
• β: 99.6841 ± 0.0019°
• γ: 95.3548 ± 0.0017°
• Cell volume: 3712.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1046
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1474
• Weighted residual factors for all reflections included in the refinement: 0.1666
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No