Information card for entry 7201605

Structure parameters

• Formula: C13 H13 N14 Zn2
• Calculated formula: C13 H11 N14 Zn2
• Title of publication: The crystal structures of four azido-bridged Zn(ii) complexes based on open-chain diazine Schiff-base ligands
• Authors of publication: Yue, Yan-Feng; Gao, En-Qing; Fang, Chen-Jie; Zheng, Tao; Liang, Jue; Yan, Chun-Hua
• Journal of publication: CrystEngComm
• Year of publication: 2008
• Journal volume: 10
• Journal issue: 5
• Pages of publication: 614
• a: 10.6683 ± 0.0002 Å
• b: 10.2683 ± 0.0002 Å
• c: 18.9476 ± 0.0007 Å
• α: 90°
• β: 117.949 ± 0.003°
• γ: 90°
• Cell volume: 1833.53 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.077
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1266
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No