Information card for entry 7202076

Structure parameters

• Formula: C31 H41 F6 P4 Rh
• Calculated formula: C31 H41 F6 P4 Rh
• Title of publication: Solid-state phosphorus-31 NMR spectroscopy of a multiple-spin system: an investigation of a rhodium‒triphosphine complex
• Authors of publication: Bernard, Guy M.; Feindel, Kirk W.; Wasylishen, Roderick E.; Cameron, T. Stanley
• Journal of publication: Physical Chemistry Chemical Physics
• Year of publication: 2008
• Journal volume: 10
• Journal issue: 36
• Pages of publication: 5552 - 5563
• a: 13.0859 ± 0.0029 Å
• b: 17.6276 ± 0.0026 Å
• c: 14.3952 ± 0.0027 Å
• α: 90°
• β: 93.396 ± 0.016°
• γ: 90°
• Cell volume: 3314.8 ± 1.1 ų
• Cell temperature: 296.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for all reflections included in the refinement: 0.1052
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No