Information card for entry 7204153

Structure parameters

• Formula: C14 H25 N Ni O5
• Calculated formula: C14 H25 N Ni O5
• SMILES: C[N](C)(CCO)[Ni]12([O]=C(C)C=C(C)O1)[O]=C(C=C(C)O2)C
• Title of publication: Synthesis and crystal structures of dimethylaminoethanol adducts of Ni(ii) acetate and Ni(ii) acetylacetonate. Precursors for the sol‒gel deposition of electrochromic nickel oxide thin films
• Authors of publication: Williams, Paul A.; Jones, Anthony C.; Bickley, Jamie F.; Steiner, Alexander; Davies, Hywel O.; Leedham, Timothy J.; Impey, Susan A.; Garcia, Joanne; Allen, Stephen; Rougier, Aline; Blyr, Alexandra
• Journal of publication: Journal of Materials Chemistry
• Year of publication: 2001
• Journal volume: 11
• Journal issue: 9
• Pages of publication: 2329
• a: 7.737 ± 0.008 Å
• b: 10.309 ± 0.007 Å
• c: 11.812 ± 0.008 Å
• α: 105.97 ± 0.08°
• β: 104.33 ± 0.11°
• γ: 97.56 ± 0.11°
• Cell volume: 857.2 ± 1.4 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1063
• Weighted residual factors for all reflections included in the refinement: 0.1141
• Goodness-of-fit parameter for all reflections included in the refinement: 0.925
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No