Information card for entry 7204154

Structure parameters

• Formula: C12 H28 N2 Ni O6
• Calculated formula: C12 H28 N2 Ni O6
• SMILES: C(C[N](C)(C)[Ni]([N](CCO)(C)C)(OC(=O)C)OC(=O)C)O
• Title of publication: Synthesis and crystal structures of dimethylaminoethanol adducts of Ni(ii) acetate and Ni(ii) acetylacetonate. Precursors for the sol‒gel deposition of electrochromic nickel oxide thin films
• Authors of publication: Williams, Paul A.; Jones, Anthony C.; Bickley, Jamie F.; Steiner, Alexander; Davies, Hywel O.; Leedham, Timothy J.; Impey, Susan A.; Garcia, Joanne; Allen, Stephen; Rougier, Aline; Blyr, Alexandra
• Journal of publication: Journal of Materials Chemistry
• Year of publication: 2001
• Journal volume: 11
• Journal issue: 9
• Pages of publication: 2329
• a: 8.2993 ± 0.0014 Å
• b: 8.5256 ± 0.0014 Å
• c: 13.017 ± 0.002 Å
• α: 95.917 ± 0.019°
• β: 95.92 ± 0.02°
• γ: 109.469 ± 0.019°
• Cell volume: 854.4 ± 0.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0473
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.0727
• Weighted residual factors for all reflections included in the refinement: 0.0755
• Goodness-of-fit parameter for all reflections included in the refinement: 0.914
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No