Information card for entry 7204351

Structure parameters

• Formula: C12 H23 Cl Sn
• Calculated formula: C12 H23 Cl Sn
• SMILES: [Sn](Cl)([C@@H]1[C@@]2(CC[C@H](C1)C2(C)C)C)(C)C
• Title of publication: Synthesis of chiral organotin reagents: synthesis of enantiomerically enriched bicyclo[2.2.1]hept-2-yl tin hydrides from camphor. X-Ray crystal structures of (dimethyl)[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]tin chloride and methyl(phenyl)bis[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]stannane
• Authors of publication: Helliwell, Madeleine; Thomas, Eric J.; Townsend, Linda A.
• Journal of publication: Journal of the Chemical Society, Perkin Transactions 1
• Year of publication: 2002
• Journal issue: 10
• Pages of publication: 1286
• a: 6.696 ± 0.007 Å
• b: 10.816 ± 0.008 Å
• c: 9.659 ± 0.007 Å
• α: 90°
• β: 93.54 ± 0.07°
• γ: 90°
• Cell volume: 698.2 ± 1 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1071
• Residual factor for significantly intense reflections: 0.0714
• Weighted residual factors for all reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.0423
• Goodness-of-fit parameter for all reflections: 2.607
• Goodness-of-fit parameter for significantly intense reflections: 2.97
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No