Information card for entry 7208196

Structure parameters

• Formula: C8 H26 Dy N6 S4 Sb
• Calculated formula: C8 H26 Dy N6 S4 Sb
• SMILES: C1C[NH]2CC[NH2][Dy]3452([NH2]1)(S[Sb](=S)(S5)[S-])[NH2]CC[NH]3CC[NH2]4
• Title of publication: Solvothermal syntheses and characterizations of lanthanide(iii)/SbS43− complexes associated by a dien ligand: A detailed study based on the lanthanide contraction effect
• Authors of publication: Tang, Weiwei; Chen, Ruihong; Zhao, Jing; Jiang, Wenqing; Zhang, Yong; Jia, Dingxian
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 15
• Pages of publication: 5021
• a: 15.82 ± 0.003 Å
• b: 9.1718 ± 0.0014 Å
• c: 13.531 ± 0.002 Å
• α: 90°
• β: 108.997 ± 0.004°
• γ: 90°
• Cell volume: 1856.4 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0617
• Weighted residual factors for all reflections included in the refinement: 0.0627
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No