Information card for entry 7208197

Structure parameters

• Common name: [Ni(en)(tren)]4Sb14S25
• Formula: C32 H104 N24 Ni4 S25 Sb14
• Calculated formula: C32 H104 N24 Ni4 S25 Sb14
• Title of publication: Using a Ni2+ complex as a structure-directing molecule: solvothermal synthesis and properties of [Ni(en)(tren)]4Sb14S25 featuring an unprecedented three-dimensional network architecture
• Authors of publication: Seidlhofer, Beatrix; Näther, Christian; Bensch, Wolfgang
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 17
• Pages of publication: 5441
• a: 16.5428 ± 0.0003 Å
• b: 25.8974 ± 0.0004 Å
• c: 22.5225 ± 0.0004 Å
• α: 90°
• β: 98.881 ± 0.001°
• γ: 90°
• Cell volume: 9533.3 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.0763
• Weighted residual factors for all reflections included in the refinement: 0.08
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No