Information card for entry 7208683

Structure parameters

• Common name: (Ni(Ni(bpy)(solv))8(W(CN)8)6).11H2O
• Chemical name: {Ni[Ni(bpy)(solv)]8[W(CN)8]6}.11H2O
• Formula: C134.4 H114.8 N64 Ni9 O19 W6
• Calculated formula: C134.4 H80 N64 Ni9 O19 W6
• Title of publication: Geometrical isomerism in pentadecanuclear high-spin Ni9W6 clusters with symmetrical bidentate ligands detected
• Authors of publication: Nowicka, Beata; Stadnicka, Katarzyna; Nitek, Wojciech; Rams, Michał; Sieklucka, Barbara
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 20
• Pages of publication: 6559
• a: 18.4747 ± 0.0011 Å
• b: 18.5055 ± 0.0012 Å
• c: 27.732 ± 0.002 Å
• α: 84.222 ± 0.003°
• β: 85.211 ± 0.004°
• γ: 87.182 ± 0.003°
• Cell volume: 9392.1 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1432
• Residual factor for significantly intense reflections: 0.1125
• Weighted residual factors for significantly intense reflections: 0.2804
• Weighted residual factors for all reflections included in the refinement: 0.304
• Goodness-of-fit parameter for all reflections included in the refinement: 1.141
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No