Information card for entry 7212837

Structure parameters

• Formula: C78 H81 Cl4 N27 O20 Pb2
• Calculated formula: C78 H81 Cl4 N27 O20 Pb2
• Title of publication: Lead(ii) complexes of bis- and tris-bidentate compartmental ligands based on pyridyl-pyrazole and pyridyl-triazole fragments: coordination networks and a discrete dimeric box
• Authors of publication: Najar, Adel M.; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 11
• Pages of publication: 3642
• a: 12.6145 ± 0.0005 Å
• b: 14.4977 ± 0.0006 Å
• c: 28.1911 ± 0.0011 Å
• α: 78.018 ± 0.002°
• β: 81.577 ± 0.002°
• γ: 79.422 ± 0.002°
• Cell volume: 4926 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.077
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1132
• Weighted residual factors for all reflections included in the refinement: 0.121
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No