Information card for entry 7212838

Structure parameters

• Formula: C44 H36 Cl2 N16 O8 Pb
• Calculated formula: C44 H36 Cl2 N16 O8 Pb
• Title of publication: Lead(ii) complexes of bis- and tris-bidentate compartmental ligands based on pyridyl-pyrazole and pyridyl-triazole fragments: coordination networks and a discrete dimeric box
• Authors of publication: Najar, Adel M.; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 11
• Pages of publication: 3642
• a: 14.2078 ± 0.0005 Å
• b: 15.0213 ± 0.0006 Å
• c: 15.6798 ± 0.0006 Å
• α: 117.794 ± 0.002°
• β: 90.479 ± 0.002°
• γ: 116.858 ± 0.002°
• Cell volume: 2537.23 ± 0.19 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1093
• Residual factor for significantly intense reflections: 0.0976
• Weighted residual factors for significantly intense reflections: 0.2187
• Weighted residual factors for all reflections included in the refinement: 0.2245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No