Structural and conformational studies of alcohol, diol and methyl ether derivatives of dibenzo-14-crown-4. Implications for ligand and tecton design
Authors of publication
Olsher, Uriel; Shoham, Gil; Dalley, N. Kent; Weining, Jiang; Luboch, Elzbieta; Yu, Zong-Yuan; Knobeloch, John M.; Lee, Jong Chan; Talanov, Vladimir S.; Bartsch, Richard A.
Journal of publication
Journal of the Chemical Society, Perkin Transactions 2
Year of publication
1999
Journal issue
11
Pages of publication
2557
a
20.295 ± 0.006 Å
b
8.139 ± 0.003 Å
c
11.205 ± 0.005 Å
α
90°
β
101.19 ± 0.02°
γ
90°
Cell volume
1815.7 ± 1.2 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
3
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1595
Residual factor for significantly intense reflections
0.0676
Weighted residual factors for all reflections
0.1747
Weighted residual factors for significantly intense reflections
0.1264
Goodness-of-fit parameter for all reflections
1.032
Goodness-of-fit parameter for significantly intense reflections
