Information card for entry 7218175

Structure parameters

• Chemical name: [N-(2-pyridinyle)diphenylephosphinic amide-kappa-O chlorotriphenyltin(IV)]
• Formula: C35 H30 Cl N2 O P Sn
• Calculated formula: C35 H30 Cl N2 O P Sn
• Title of publication: Steric and electronic control over the structural diversity of N-(n-pyridinyl) diphenylphosphinic amides (n = 2 and 4) as difunctional ligands in triphenyltin(iv) adducts
• Authors of publication: Gholivand, K.; Gholami, A.; Tizhoush, S. K.; Schenk, K. J.; Fadaei, F.; Bahrami, A.
• Journal of publication: RSC Adv.
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 84
• Pages of publication: 44509
• a: 57.264 ± 0.002 Å
• b: 9.8858 ± 0.0002 Å
• c: 22.2965 ± 0.0008 Å
• α: 90°
• β: 93.908 ± 0.003°
• γ: 90°
• Cell volume: 12592.7 ± 0.7 ų
• Cell temperature: 292 ± 2 K
• Ambient diffraction temperature: 292 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/n 1
• Hall space group symbol: -C 2yac
• Residual factor for all reflections: 0.0377
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0602
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No