Information card for entry 7221596

Structure parameters

• Formula: C37 H32 Cl2 N2 Ni O2
• Calculated formula: C37 H32 Cl2 N2 Ni O2
• Title of publication: Synthesis of well defined C‒C bridged Ni(ii) complexes bearing β-ketoiminato-fluorene ligands by bifluorenyl in situ coupling and application for norbornene (co)polymerization
• Authors of publication: Tian, Jianwen; He, Xiaohui; Liu, Jingyin; Deng, Xiaodan; Chen, Defu
• Journal of publication: RSC Adv.
• Year of publication: 2015
• Journal volume: 5
• Journal issue: 76
• Pages of publication: 61851
• a: 9.0438 ± 0.0008 Å
• b: 19.4513 ± 0.0018 Å
• c: 18.124 ± 0.0017 Å
• α: 90°
• β: 96.817 ± 0.001°
• γ: 90°
• Cell volume: 3165.7 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1007
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.1735
• Weighted residual factors for all reflections included in the refinement: 0.2031
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No