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Information card for entry 7221597
Preview
Coordinates | 7221597.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37 H26 Cl2 F6 N2 Ni O2 |
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Calculated formula | C37 H26 Cl2 F6 N2 Ni O2 |
SMILES | [Ni]123[N](=C(C)C=C(C(F)(F)F)O2)C2(c4ccccc4c4ccccc24)C2(c4ccccc4c4ccccc24)[N]1=C(C)C=C(C(F)(F)F)O3.C(Cl)Cl |
Title of publication | Synthesis of well defined C‒C bridged Ni(ii) complexes bearing β-ketoiminato-fluorene ligands by bifluorenyl in situ coupling and application for norbornene (co)polymerization |
Authors of publication | Tian, Jianwen; He, Xiaohui; Liu, Jingyin; Deng, Xiaodan; Chen, Defu |
Journal of publication | RSC Adv. |
Year of publication | 2015 |
Journal volume | 5 |
Journal issue | 76 |
Pages of publication | 61851 |
a | 9.1247 ± 0.0018 Å |
b | 22.75 ± 0.005 Å |
c | 16.595 ± 0.003 Å |
α | 90° |
β | 103.533 ± 0.002° |
γ | 90° |
Cell volume | 3349.3 ± 1.2 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0585 |
Residual factor for significantly intense reflections | 0.0516 |
Weighted residual factors for significantly intense reflections | 0.1379 |
Weighted residual factors for all reflections included in the refinement | 0.1455 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.047 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7221597.html
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