Information card for entry 7222479

Structure parameters

• Formula: C80 H113 Cl2 N O7 V2
• Calculated formula: C80 H113 Cl2 N O7 V2
• Title of publication: Vanadium(V) tetra-phenolate complexes: Synthesis, structural studies and ethylene homo-(co-)polymerization capability
• Authors of publication: Redshaw, Carl; Walton, Mark; Elsegood, Mark Robert James; Prior, Timothy J.; Michiue, Kenji
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 9.446 ± 0.0006 Å
• b: 11.18 ± 0.0007 Å
• c: 19.3754 ± 0.0013 Å
• α: 77.635 ± 0.004°
• β: 81.522 ± 0.004°
• γ: 85.307 ± 0.005°
• Cell volume: 1974.2 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2135
• Residual factor for significantly intense reflections: 0.0895
• Weighted residual factors for significantly intense reflections: 0.1929
• Weighted residual factors for all reflections included in the refinement: 0.2553
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No