Information card for entry 7222480

Structure parameters

• Formula: C80 H108 Cl2 F3 N O7 V2
• Calculated formula: C80 H108 Cl2 F3 N O7 V2
• Title of publication: Vanadium(V) tetra-phenolate complexes: Synthesis, structural studies and ethylene homo-(co-)polymerization capability
• Authors of publication: Redshaw, Carl; Walton, Mark; Elsegood, Mark Robert James; Prior, Timothy J.; Michiue, Kenji
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 9.413 ± 0.007 Å
• b: 11.244 ± 0.008 Å
• c: 19.369 ± 0.013 Å
• α: 79.2 ± 0.04°
• β: 80.9 ± 0.03°
• γ: 84.4 ± 0.04°
• Cell volume: 1983 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1424
• Residual factor for significantly intense reflections: 0.1053
• Weighted residual factors for significantly intense reflections: 0.253
• Weighted residual factors for all reflections included in the refinement: 0.2815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No