Information card for entry 7222481

Structure parameters

• Formula: C114 H132 Cl2 N2 O6 V2
• Calculated formula: C114 H132 Cl2 N2 O6 V2
• Title of publication: Vanadium(V) tetra-phenolate complexes: Synthesis, structural studies and ethylene homo-(co-)polymerization capability
• Authors of publication: Redshaw, Carl; Walton, Mark; Elsegood, Mark Robert James; Prior, Timothy J.; Michiue, Kenji
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 10.8048 ± 0.0012 Å
• b: 14.4744 ± 0.0013 Å
• c: 18.3207 ± 0.0019 Å
• α: 74.937 ± 0.008°
• β: 84.606 ± 0.009°
• γ: 69.796 ± 0.008°
• Cell volume: 2596.5 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1577
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1407
• Weighted residual factors for all reflections included in the refinement: 0.1661
• Goodness-of-fit parameter for all reflections included in the refinement: 0.785
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No