Information card for entry 7223494

Structure parameters

• Formula: C71 H104 Ge2 N8 S2 Si4
• Calculated formula: C71 H104 Ge2 N8 S2 Si4
• Title of publication: Mixed guanidinato-amido Ge(IV) and Sn(IV) complexes with Ge=E (E = S, Se) double bond and SnS4, Sn2Se2 rings†
• Authors of publication: Barman, Milan Kumar; Nembenna, Sharanappa
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 37.184 ± 0.005 Å
• b: 10.465 ± 0.005 Å
• c: 26.604 ± 0.005 Å
• α: 90 ± 0.005°
• β: 131.927 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 7702 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.092
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.1663
• Weighted residual factors for all reflections included in the refinement: 0.1882
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No