Information card for entry 7224307

Structure parameters

• Formula: C22 H33 B Br3 Ge N3
• Calculated formula: C22 H33 B Br3 Ge N3
• SMILES: Br[Ge](Br)(Br)N(B(Nc1c(cccc1C)C)N(C(C)C)C(C)C)c1c(cccc1C)C
• Title of publication: Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand
• Authors of publication: Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; Růžička, Aleš; Dostál, Libor
• Journal of publication: RSC Adv.
• Year of publication: 2016
• Journal volume: 6
• Journal issue: 23
• Pages of publication: 19377
• a: 9.48 ± 0.003 Å
• b: 9.529 ± 0.0011 Å
• c: 31.902 ± 0.006 Å
• α: 86.052 ± 0.012°
• β: 86.293 ± 0.016°
• γ: 65.709 ± 0.016°
• Cell volume: 2618.4 ± 1.1 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1052
• Residual factor for significantly intense reflections: 0.086
• Weighted residual factors for significantly intense reflections: 0.1899
• Weighted residual factors for all reflections included in the refinement: 0.2011
• Goodness-of-fit parameter for all reflections included in the refinement: 1.281
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No