Information card for entry 7224308

Structure parameters

• Formula: C22 H33 B Br Ge N3
• Calculated formula: C22 H33 B Br Ge N3
• SMILES: [Ge]1(Br)N(B(N(C(C)C)C(C)C)[NH]1c1c(C)cccc1C)c1c(C)cccc1C
• Title of publication: Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand
• Authors of publication: Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; Růžička, Aleš; Dostál, Libor
• Journal of publication: RSC Adv.
• Year of publication: 2016
• Journal volume: 6
• Journal issue: 23
• Pages of publication: 19377
• a: 8.352 ± 0.0004 Å
• b: 10.479 ± 0.0005 Å
• c: 13.5181 ± 0.001 Å
• α: 95.684 ± 0.005°
• β: 100.864 ± 0.006°
• γ: 90.338 ± 0.004°
• Cell volume: 1155.83 ± 0.12 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0477
• Residual factor for significantly intense reflections: 0.0306
• Weighted residual factors for significantly intense reflections: 0.0627
• Weighted residual factors for all reflections included in the refinement: 0.0703
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No