Information card for entry 7226798

Structure parameters

• Formula: Ge4 Na9 S12 Sb
• Calculated formula: Ge4 Na9 S12 Sb
• Title of publication: Na9Sb(Ge2Q6)2 (Q = S, Se): two new antimony (III) quaternary chalcogenides with ethane-like [Ge2Q6]6− ligands
• Authors of publication: Wu, Xiaowen; Hu, Yi; Pan, Hui; Su, Zhi
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 7.5857 ± 0.0007 Å
• b: 11.5743 ± 0.0011 Å
• c: 6.8175 ± 0.0011 Å
• α: 90°
• β: 106.587 ± 0.003°
• γ: 90°
• Cell volume: 573.66 ± 0.12 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0212
• Residual factor for significantly intense reflections: 0.0184
• Weighted residual factors for significantly intense reflections: 0.0421
• Weighted residual factors for all reflections included in the refinement: 0.0429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No