Information card for entry 7226799

Structure parameters

• Formula: Ge4 Na9 Sb Se12
• Calculated formula: Ge4 Na9 Sb Se12
• Title of publication: Na9Sb(Ge2Q6)2 (Q = S, Se): two new antimony (III) quaternary chalcogenides with ethane-like [Ge2Q6]6− ligands
• Authors of publication: Wu, Xiaowen; Hu, Yi; Pan, Hui; Su, Zhi
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 8.95 ± 0.01 Å
• b: 24.33 ± 0.03 Å
• c: 7.066 ± 0.008 Å
• α: 90°
• β: 122.103 ± 0.011°
• γ: 90°
• Cell volume: 1303 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1208
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.1193
• Weighted residual factors for all reflections included in the refinement: 0.1462
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No