Information card for entry 7227275

Structure parameters

• Formula: C25 H44 Lu N3 Si2
• Calculated formula: C25 H44 Lu N3 Si2
• SMILES: [Lu]123456(N(CC[c]76[cH]2[cH]1[c]15cccc[c]471)[C@H]1[C@H]([N]3(C)C)CCCC1)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Half-Sandwich Chiral Rare-Earth Metal Complexes with Linked Tridentate Amido-Indenyl Ligand: Synthesis, Characterization, and Catalytic Properties for Intramolecular Hydroamination
• Authors of publication: Chai, Zhuo; Chu, Jiang; Qi, Yunyi; Tang, Mujun; Hou, Jinsong; Yang, Gaosheng
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 8.9592 ± 0.0012 Å
• b: 10.1194 ± 0.0013 Å
• c: 15.698 ± 0.002 Å
• α: 90°
• β: 98.047 ± 0.001°
• γ: 90°
• Cell volume: 1409.2 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0225
• Residual factor for significantly intense reflections: 0.0204
• Weighted residual factors for significantly intense reflections: 0.0467
• Weighted residual factors for all reflections included in the refinement: 0.0477
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No