Information card for entry 7230386

Structure parameters

• Formula: C24 H33 N2 O7 P S
• Calculated formula: C24 H33 N2 O7 P S
• Title of publication: Functionalization of α-hydroxyphosphonates as a convenient route to N-tosyl-α-aminophosphonates
• Authors of publication: Cytlak, Tomasz; Skibińska, Monika; Kaczmarek, Patrycja; Kaźmierczak, Marcin; Rapp, Magdalena; Kubicki, Maciej; Koroniak, Henryk
• Journal of publication: RSC Advances
• Year of publication: 2018
• Journal volume: 8
• Journal issue: 22
• Pages of publication: 11957
• a: 9.1196 ± 0.0007 Å
• b: 11.0522 ± 0.0009 Å
• c: 13.648 ± 0.0013 Å
• α: 71.568 ± 0.008°
• β: 77.69 ± 0.007°
• γ: 87.393 ± 0.006°
• Cell volume: 1274.7 ± 0.2 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1169
• Residual factor for significantly intense reflections: 0.0851
• Weighted residual factors for significantly intense reflections: 0.1902
• Weighted residual factors for all reflections included in the refinement: 0.205
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No