Crystallography Open Database

Information card for entry 7230387

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Coordinates	7230387.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H28 F3 N2 O5 P S
Calculated formula	C22 H28 F3 N2 O5 P S
Title of publication	Functionalization of α-hydroxyphosphonates as a convenient route to N-tosyl-α-aminophosphonates
Authors of publication	Cytlak, Tomasz; Skibińska, Monika; Kaczmarek, Patrycja; Kaźmierczak, Marcin; Rapp, Magdalena; Kubicki, Maciej; Koroniak, Henryk
Journal of publication	RSC Advances
Year of publication	2018
Journal volume	8
Journal issue	22
Pages of publication	11957
a	9.4187 ± 0.0003 Å
b	11.5503 ± 0.0005 Å
c	25.4175 ± 0.001 Å
α	90.406 ± 0.003°
β	99.189 ± 0.003°
γ	113.524 ± 0.004°
Cell volume	2495.13 ± 0.19 Å³
Cell temperature	130 ± 1 K
Ambient diffraction temperature	130 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0529
Residual factor for significantly intense reflections	0.0408
Weighted residual factors for significantly intense reflections	0.0987
Weighted residual factors for all reflections included in the refinement	0.1063
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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