A chiral spiroborate anion from diphenyl-l-tartramide [B{l-Tar(NHPh)2}2]−applied to some challenging resolutions
Authors of publication
Wong, Lawrence W.-Y.; Tam, Gemma S.-S.; Chen, Xiaoyan; So, Frederick T.-K.; Soecipto, Aristyo; Sheong, Fu Kit; Sung, Herman H.-Y.; Lin, Zhenyang; Williams, Ian D.
Journal of publication
CrystEngComm
Year of publication
2018
Journal volume
20
Journal issue
33
Pages of publication
4831
a
9.453 ± 0.003 Å
b
40.907 ± 0.005 Å
c
9.917 ± 0.003 Å
α
90°
β
91.57 ± 0.02°
γ
90°
Cell volume
3833.4 ± 1.7 Å3
Cell temperature
248 K
Ambient diffraction temperature
248 K
Number of distinct elements
4
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.049
Residual factor for significantly intense reflections
0.041
Weighted residual factors for all reflections included in the refinement
0.122
Goodness-of-fit parameter for all reflections included in the refinement