A chiral spiroborate anion from diphenyl-l-tartramide [B{l-Tar(NHPh)2}2]−applied to some challenging resolutions
Authors of publication
Wong, Lawrence W.-Y.; Tam, Gemma S.-S.; Chen, Xiaoyan; So, Frederick T.-K.; Soecipto, Aristyo; Sheong, Fu Kit; Sung, Herman H.-Y.; Lin, Zhenyang; Williams, Ian D.
Journal of publication
CrystEngComm
Year of publication
2018
Journal volume
20
Journal issue
33
Pages of publication
4831
a
5.51895 ± 0.00007 Å
b
15.5145 ± 0.0002 Å
c
22.2271 ± 0.0003 Å
α
90°
β
94.4499 ± 0.0012°
γ
90°
Cell volume
1897.43 ± 0.04 Å3
Cell temperature
100.01 ± 0.1 K
Ambient diffraction temperature
100.01 ± 0.1 K
Number of distinct elements
5
Space group number
4
Hermann-Mauguin space group symbol
P 1 21 1
Hall space group symbol
P 2yb
Residual factor for all reflections
0.0434
Residual factor for significantly intense reflections
0.0414
Weighted residual factors for significantly intense reflections
0.1029
Weighted residual factors for all reflections included in the refinement
0.1045
Goodness-of-fit parameter for all reflections included in the refinement
