Information card for entry 7232254

Structure parameters

• Formula: C26 H28 N2 Ni O4
• Calculated formula: C26 H28 N2 Ni O4
• Title of publication: Synthesis and characterisation of κ2-N,O-oxazoline-enolate complexes of nickel(ii): explorations in coordination chemistry and metal-mediated polymerisation
• Authors of publication: Adjei, Jeanette A.; Lough, Alan J.; Gossage, Robert A.
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 7
• Pages of publication: 3956
• a: 12.0764 ± 0.0017 Å
• b: 9.6715 ± 0.0015 Å
• c: 20.657 ± 0.004 Å
• α: 90°
• β: 92.155 ± 0.005°
• γ: 90°
• Cell volume: 2411 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0928
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0868
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No