Information card for entry 7232255

Structure parameters

• Formula: C22 H24 N2 Ni O6
• Calculated formula: C22 H24 N2 Ni O6
• Title of publication: Synthesis and characterisation of κ2-N,O-oxazoline-enolate complexes of nickel(ii): explorations in coordination chemistry and metal-mediated polymerisation
• Authors of publication: Adjei, Jeanette A.; Lough, Alan J.; Gossage, Robert A.
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 7
• Pages of publication: 3956
• a: 10.2574 ± 0.0008 Å
• b: 8.8952 ± 0.0007 Å
• c: 23.418 ± 0.002 Å
• α: 90°
• β: 95.19 ± 0.003°
• γ: 90°
• Cell volume: 2127.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0548
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0643
• Weighted residual factors for all reflections included in the refinement: 0.0714
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No