Information card for entry 7232256

Structure parameters

• Formula: C26 H26 N4 Ni O8
• Calculated formula: C26 H26 N4 Ni O8
• Title of publication: Synthesis and characterisation of κ2-N,O-oxazoline-enolate complexes of nickel(ii): explorations in coordination chemistry and metal-mediated polymerisation
• Authors of publication: Adjei, Jeanette A.; Lough, Alan J.; Gossage, Robert A.
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 7
• Pages of publication: 3956
• a: 9.5476 ± 0.001 Å
• b: 10.5561 ± 0.0012 Å
• c: 14.4705 ± 0.0016 Å
• α: 74.72 ± 0.003°
• β: 70.961 ± 0.003°
• γ: 70.689 ± 0.003°
• Cell volume: 1281.1 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0681
• Weighted residual factors for all reflections included in the refinement: 0.0733
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No