Information card for entry 7235279

Structure parameters

• Formula: C83.9 H58 N17.6 Ni3 O8.9
• Calculated formula: C83.9 H57.6 N17.6 Ni3 O8.9
• Title of publication: An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
• Authors of publication: Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 32
• Pages of publication: 13214
• a: 14.565 ± 0.007 Å
• b: 15.905 ± 0.007 Å
• c: 16.366 ± 0.008 Å
• α: 85.02 ± 0.05°
• β: 88.64 ± 0.05°
• γ: 73.41 ± 0.05°
• Cell volume: 3620 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.4374
• Residual factor for significantly intense reflections: 0.1214
• Weighted residual factors for significantly intense reflections: 0.1253
• Weighted residual factors for all reflections included in the refinement: 0.2189
• Goodness-of-fit parameter for all reflections included in the refinement: 0.932
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No