Information card for entry 7235280

Structure parameters

• Formula: C101.5 H74.6 N18 Ni6 O18.8
• Calculated formula: C101.5 H72 N18 Ni6 O18.8
• Title of publication: An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
• Authors of publication: Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 32
• Pages of publication: 13214
• a: 17.036 ± 0.007 Å
• b: 17.422 ± 0.007 Å
• c: 19.4 ± 0.008 Å
• α: 64.27 ± 0.04°
• β: 77.69 ± 0.03°
• γ: 63.98 ± 0.04°
• Cell volume: 4659 ± 4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2115
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.0485
• Weighted residual factors for all reflections included in the refinement: 0.0599
• Goodness-of-fit parameter for all reflections included in the refinement: 0.889
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No