Information card for entry 7235281

Structure parameters

• Formula: C102.8 H105 Cl N18 Ni5 O27.2
• Calculated formula: C102.8 H102.2 Cl N18 Ni5 O27.2
• Title of publication: An indeno-quinoxaline based oxime ligand for the synthesis of polynuclear Ni(ii) clusters
• Authors of publication: Canaj, Angelos B.; Nodaraki, Lydia E.; Philippidis, Aggelos; Tzimopoulos, Demetrios I.; Fotopoulou, Eirini; Siczek, Milosz; Lis, Tadeusz; Milios, Constantinos J.
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 32
• Pages of publication: 13214
• a: 15.782 ± 0.004 Å
• b: 17.617 ± 0.005 Å
• c: 19.885 ± 0.005 Å
• α: 93.8 ± 0.03°
• β: 100.35 ± 0.03°
• γ: 97 ± 0.03°
• Cell volume: 5376 ± 3 ų
• Cell temperature: 80 ± 2 K
• Ambient diffraction temperature: 80 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1068
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1664
• Weighted residual factors for all reflections included in the refinement: 0.2008
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No