Information card for entry 7236021

Structure parameters

• Formula: C40 H48 Cl4 F6 N2 P Sb
• Calculated formula: C40 H48 Cl4 F6 N2 P Sb
• Title of publication: Hypervalent diorganoantimony(iii) fluorides via diorganoantimony(iii) cations ‒ a general method of synthesis
• Authors of publication: Preda, Ana Maria; Raţ, Ciprian I.; Silvestru, Cristian; Lang, Heinrich; Rüffer, Tobias; Mehring, Michael
• Journal of publication: RSC Advances
• Year of publication: 2015
• Journal volume: 5
• Journal issue: 121
• Pages of publication: 99832
• a: 10.3364 ± 0.0004 Å
• b: 24.8372 ± 0.0007 Å
• c: 16.7958 ± 0.0005 Å
• α: 90°
• β: 98.284 ± 0.003°
• γ: 90°
• Cell volume: 4266.9 ± 0.2 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0721
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.0784
• Goodness-of-fit parameter for all reflections included in the refinement: 0.84
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No