Information card for entry 7236022

Structure parameters

• Formula: C34 H34 Cl6 F6 N2 P Sb
• Calculated formula: C34 H34 Cl6 F6 N2 P Sb
• Title of publication: Hypervalent diorganoantimony(iii) fluorides via diorganoantimony(iii) cations ‒ a general method of synthesis
• Authors of publication: Preda, Ana Maria; Raţ, Ciprian I.; Silvestru, Cristian; Lang, Heinrich; Rüffer, Tobias; Mehring, Michael
• Journal of publication: RSC Advances
• Year of publication: 2015
• Journal volume: 5
• Journal issue: 121
• Pages of publication: 99832
• a: 12.2715 ± 0.0012 Å
• b: 12.4401 ± 0.0009 Å
• c: 15.1691 ± 0.001 Å
• α: 80.778 ± 0.006°
• β: 71.653 ± 0.008°
• γ: 70.246 ± 0.008°
• Cell volume: 2064.9 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0698
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1489
• Weighted residual factors for all reflections included in the refinement: 0.1521
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No