Information card for entry 7238514

Structure parameters

• Common name: (Co(N4C6H18)(H2O))3V15Sb6O42(H2O)H2O
• Formula: C18 H58 Co3 N12 O47 Sb6 V15
• Calculated formula: C18 H54 Co3 N12 O47.6 Sb6 V15
• Title of publication: Assembly of [V15Sb6O42(H2O)]6− cluster shells into higher dimensional aggregates via weak Sb⋯N/Sb⋯O intercluster interactions and a new polyoxovanadate with a discrete [V16Sb4O42(H2O)]8− cluster shell
• Authors of publication: Antonova, Elena; Näther, Christian; Bensch, Wolfgang
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 20
• Pages of publication: 6853
• a: 12.3811 ± 0.0005 Å
• b: 12.3811 ± 0.0005 Å
• c: 41.398 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5495.8 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.0355
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No