Information card for entry 7238515

Structure parameters

• Formula: C62 H214 Co6 N42 O97 Sb12 V30
• Calculated formula: C62 H188 Co6 N42 O97 Sb12 V30
• Title of publication: Assembly of [V15Sb6O42(H2O)]6− cluster shells into higher dimensional aggregates via weak Sb⋯N/Sb⋯O intercluster interactions and a new polyoxovanadate with a discrete [V16Sb4O42(H2O)]8− cluster shell
• Authors of publication: Antonova, Elena; Näther, Christian; Bensch, Wolfgang
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 20
• Pages of publication: 6853
• a: 27.8795 ± 0.0011 Å
• b: 22.9567 ± 0.0009 Å
• c: 32.2932 ± 0.0013 Å
• α: 90°
• β: 113.717 ± 0.004°
• γ: 90°
• Cell volume: 18922.8 ± 1.4 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1198
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 0.966
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No