Information card for entry 7238793

Structure parameters

• Formula: C37 H34 F24 N4 O P4
• Calculated formula: C37 H34 F24 N4 O P4
• Title of publication: Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling
• Authors of publication: Xi, Hai-Tao; Zhao, Ting; Sun, Xiao-Qiang; Miao, Chun-Bao; Zong, Ting; Meng, Qi
• Journal of publication: RSC Adv.
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 3
• Pages of publication: 691
• a: 7.692 ± 0.003 Å
• b: 20.23 ± 0.007 Å
• c: 14.097 ± 0.005 Å
• α: 90°
• β: 94.13 ± 0.009°
• γ: 90°
• Cell volume: 2187.9 ± 1.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2205
• Residual factor for significantly intense reflections: 0.0744
• Weighted residual factors for significantly intense reflections: 0.1323
• Weighted residual factors for all reflections included in the refinement: 0.1699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No