Information card for entry 7238794

Structure parameters

• Formula: C37 H35 F24 N5 O7 P4
• Calculated formula: C37 H35 F24 N5 O7 P4
• Title of publication: Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling
• Authors of publication: Xi, Hai-Tao; Zhao, Ting; Sun, Xiao-Qiang; Miao, Chun-Bao; Zong, Ting; Meng, Qi
• Journal of publication: RSC Adv.
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 3
• Pages of publication: 691
• a: 10.0819 ± 0.0018 Å
• b: 10.9811 ± 0.0019 Å
• c: 14.025 ± 0.003 Å
• α: 68.984 ± 0.005°
• β: 76.417 ± 0.005°
• γ: 79.993 ± 0.005°
• Cell volume: 1402 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.2429
• Residual factor for significantly intense reflections: 0.1188
• Weighted residual factors for significantly intense reflections: 0.2914
• Weighted residual factors for all reflections included in the refinement: 0.3799
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No