Information card for entry 7239058

Structure parameters

• Formula: C16 H25 Cu4 N12 O41 P W12
• Calculated formula: C16 H24 Cu4 N12 O41 P W12
• Title of publication: Hydroxyl- and chloro-bridges as “structural assistants” in the construction of two new Keggin-based 3D frameworks
• Authors of publication: Tian, AiXiang; Lin, XiaoLing; Liu, XiaoJing; Ying, Jun; Wang, XiuLi
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 38
• Pages of publication: 17188
• a: 12.774 ± 0.005 Å
• b: 19.299 ± 0.005 Å
• c: 11.056 ± 0.005 Å
• α: 90°
• β: 98.752 ± 0.005°
• γ: 90°
• Cell volume: 2693.8 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0463
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.1048
• Weighted residual factors for all reflections included in the refinement: 0.1108
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No