Information card for entry 7239059

Structure parameters

• Formula: C32 H54 Cl Cu2 N24 O43 P W12
• Calculated formula: C32 H48 Cl Cu2 N24 O43 P W12
• Title of publication: Hydroxyl- and chloro-bridges as “structural assistants” in the construction of two new Keggin-based 3D frameworks
• Authors of publication: Tian, AiXiang; Lin, XiaoLing; Liu, XiaoJing; Ying, Jun; Wang, XiuLi
• Journal of publication: RSC Advances
• Year of publication: 2013
• Journal volume: 3
• Journal issue: 38
• Pages of publication: 17188
• a: 12.067 ± 0.005 Å
• b: 15.262 ± 0.005 Å
• c: 20.31 ± 0.005 Å
• α: 96.457 ± 0.005°
• β: 95.796 ± 0.005°
• γ: 90.465 ± 0.005°
• Cell volume: 3697 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.104
• Residual factor for significantly intense reflections: 0.0763
• Weighted residual factors for significantly intense reflections: 0.1572
• Weighted residual factors for all reflections included in the refinement: 0.1705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No